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Preparations of hydroxyapatite from tilapia scales

Sockalingam, Kanageswary and Yahya, Mohd Azha and Abdullah, Hasan Zuhudi (2014) Preparations of hydroxyapatite from tilapia scales. In: International Conference on X-Ray & Related Technique in Research and Industry (ICXRI2014), 11-13 August 2014 , Johor Bahru, Johor.

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Abstract

Hydroxyapatite (HAP), classified as bioceramic materials is the major mineral constituent of vertebrate bones and teeth. In this study, the effect of temperature on isolation and characterization of HAp from tilapia fish scales have been investigated. Scales were subjected to heat treatment at different temperatures (800°C and 1000°C) and microstructure of both raw and calcined scales were observed under Scanning Electron Microscopy (SEM). Thermo Gravimetric Analysis (TGA) and Energy Dispersive X-Ray Spectroscopy (EDX) results have revealed the'. best calcination temperature of tilapia scales to be 800°C due to the calculated calcium to phosphorous weight ratio (Ca/P). The Ca/P ratio for scales treated at 800°C and 1000°C were 1.598 and 1.939 respectively. The phase purity and crystallinity of produced HAp was further confirmed by X-Ray Diffraction (XRD) analysis. Based on the study, it can be concluded that tilapia fish scale is a good natural source of HAp with 800°C as the optimum calcination temperature in HAp production.

Item Type: Conference or Workshop Item (Paper)
Uncontrolled Keywords: hydroxyapatite; fish scale; calcination
Subjects: T Technology > TA Engineering (General). Civil engineering (General) > TA170-171 Environmental engineering
Divisions: Faculty of Mechanical and Manufacturing Engineering > Department of Materials Engineering and Design
Depositing User: Normajihan Abd. Rahman
Date Deposited: 23 Apr 2015 01:09
Last Modified: 23 Apr 2015 01:09
URI: http://eprints.uthm.edu.my/id/eprint/5898
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